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Combined Analysis of Stable Isotope, 1H NMR, and Fatty Acid To Verify Sesame Oil Authenticity

Authors
Kim, JeongeunJin, GyungsuLee, YunheeChun, Hyang SookAhn, SangdooKim, Byung Hee
Issue Date
Oct-2015
Publisher
AMER CHEMICAL SOC, 1155 16TH ST, NW, WASHINGTON, USA, DC, 20036
Citation
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, v.63, no.40, pp 8955 - 8965
Pages
11
Journal Title
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
Volume
63
Number
40
Start Page
8955
End Page
8965
URI
https://scholarworks.sookmyung.ac.kr/handle/2020.sw.sookmyung/147107
DOI
10.1021/acs.jafc.5b04082
ISSN
0021-8561
1520-5118
Abstract
The aim of this study was to verify the authenticity of sesame oils using combined analysis of stable isotope ratio, 1H NMR spectroscopy, and fatty acid profiles of the oils. Analytical data were obtained from 35 samples of authentic sesame oils and 29 samples of adulterated sesame oils currently distributed in Korea. The orthogonal projection to latent structure discriminant analysis technique was used to select variables that most effectively verify the sesame oil authenticity. The variables include δ13C value, integration values of NMR peaks that signify the CH3 of n-3 fatty acids, CH2 between two C═C, protons from sesamin/sesamolin, and 18:1n-9, 18:3n-3, 18:2t, and 18:3t content values. The authenticity of 65 of 70 blind samples was correctly verified by applying the range of the eight variables found in the authentic sesame oil samples, suggesting that triple analysis is a useful approach to verify sesame oil authenticity.
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Kim, Byung Hee
생활과학대학 (식품영양학과)
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