A Mononuclear Nonheme Iron(V)-Imido Complex
  • Hong, Seungwoo
  • Sutherlin, Kyle D.
  • Vardhaman, Anil Kumar
  • Yan, James J.
  • Park, Sora
  • 외 7명
Citations

WEB OF SCIENCE

70
Citations

SCOPUS

70

초록

Mononuclear nonheme iron(V)-oxo complexes have been reported previously. Herein, we report the first example of a mononuclear nonheme iron(V)-imido complex bearing a tetraamido macrocyclic ligand (TAML), [(TAML)Fe-V(NTs)](-) (1). The spectroscopic characterization of 1 revealed an S = 1/2 Fe(V) oxidation state, an Fe-N bond length of 1.65(4) angstrom, and an Fe-N vibration at 817 cm(-1). The reactivity of 1 was demonstrated in C-H bond functionalization and nitrene transfer reactions.

키워드

METAL-OXO COMPLEXESOXIDATION REACTIONSTRANSFER REACTIVITYIRONIRON(IV)-OXONITRIDOFEHYDROXYLATIONENVIRONMENTSAMINATION
제목
A Mononuclear Nonheme Iron(V)-Imido Complex
저자
Hong, SeungwooSutherlin, Kyle D.Vardhaman, Anil KumarYan, James J.Park, SoraLee, Yong-MinJang, SoojeongLu, XiaoyanOhta, TakehiroOgura, TakashiSolomon, Edward I.Nam, Wonwoo
DOI
10.1021/jacs.7b04695
발행일
2017-07
유형
Article
저널명
Journal of the American Chemical Society
139
26
페이지
8800 ~ 8803