Determination of seed content in red pepper powders by H-1 NMR and second-derivative FT-IR spectroscopy combined with statistical analyses
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초록

This study focuses on discriminating the seed content in red pepper powders using H-1 NMR and second-derivative FT-IR Spectroscopy with canonical discriminant and multiple linear regression analyses. We used 165 test samples prepared by varying the seed content for spectroscopic analyses. The canonical discriminant functions derived from 21 peak variables were used to properly discriminate the red pepper powder samples based on their seed content with a 97.6% hit ratio. Additionally, we observed an average error of 7.0% while discriminating 42 blind samples. Multiple linear regression analysis was performed to directly determine the seed content of new samples without running a statistical program. The best regression model constructed with only two variables showed an average error of 6.2% when applied to the blind samples. These results verify the feasibility of using H-1 NMR and FT-IR Spectroscopy with statistical analyses to determine the seed content in red pepper powders.

키워드

H-1 NMRcanonical discriminant analysismultiple linear regression analysisred pepper powdersecond derivative FT-IRseed contentFATTY-ACIDINFRARED-SPECTROSCOPYAMINO-ACIDCAPSICUMMETABOLISMPROFILESORIGINOILSMIR
제목
Determination of seed content in red pepper powders by H-1 NMR and second-derivative FT-IR spectroscopy combined with statistical analyses
저자
Choi, YuriHong, JunyoungKim, Byung HeeAhn, Sangdoo
DOI
10.1002/bkcs.12476
발행일
2022-03
유형
Article; Early Access
저널명
Bulletin of the Korean Chemical Society
43
3
페이지
450 ~ 459