Recyclable and eco-friendly Pd-complexed graphene oxide/N-heterocyclic carbene catalyst for various coupling reactions in aqueous phase
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초록

In this study, we report recyclable Pd-complexed graphene oxide (GO) catalysts with a bulky N-heterocyclic carbene (NHC) ligand (GO/NHC-Pd) for various cross-coupling reactions in the aqueous phase. To prepare GO/NHC-Pd, the NHC precursor and a trimethoxy-silane linker were combined on the GO surface via condensation, followed by the Pd chelation over GO/NHC. The GO-based catalysts were applied to three types of C-C cross-coupling reactions including Suzuki, Heck and Sonogashira reactions in the aqueous phase, to evaluate their catalytic performance. The reusability of the catalysts was tested by performing five consequent cross-coupling reactions. (C) 2017 Elsevier Ltd. All rights reserved.

키워드

Heterogeneous catalystGraphene oxideN-Heterocyclic carbenePalladiumC-C cross couplingSUZUKI-MIYAURAPALLADIUM COMPLEXGRAPHITE OXIDEMIZOROKI-HECKSONOGASHIRANANOPARTICLESCHLORIDESEFFICIENT
제목
Recyclable and eco-friendly Pd-complexed graphene oxide/N-heterocyclic carbene catalyst for various coupling reactions in aqueous phase
저자
Kim, SeongsooCho, Hong-JunShin, Dong-SikLee, Sang-Myung
DOI
10.1016/j.tetlet.2017.05.017
발행일
2017-06
유형
Article
저널명
Tetrahedron Letters
58
25
페이지
2421 ~ 2425