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Kinetic resolution of racemic 2-substituted cyclohexanones by enantioselective deprotonation
- Issue Date
- Aug-1989
- Publisher
- PERGAMON-ELSEVIER SCIENCE LTD
- Citation
- Tetrahedron Letters, v.30, no.47, pp 6537 - 6540
- Pages
- 4
- Journal Title
- Tetrahedron Letters
- Volume
- 30
- Number
- 47
- Start Page
- 6537
- End Page
- 6540
- ISSN
- 0040-4039
- Abstract
- Incomplete deprotonation of racemic 2-substituted cyclohexanones (d1-4) by chiral lithium amides (2) in the presence of trimethylsilyl chloride was found to give the corresponding trimethylsilyl enol ethers (5) and the unreacted ketones (4) in reasonably high enantiomeric excesses. Kawasaki, Hisashi
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